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Transmission electron microscopy for materials science · LearnSpace
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Transmission electron microscopy for materials science

Курс от École Polytechnique Fédérale de Lausanne
Средний≈ 45.9 чАнглийский
О курсеНавыкиПрограммаПреподаватели

О курсе

Learn about the fundamentals of transmission electron microscopy in materials sciences: you will be able to understand papers where TEM has been used and have the necessary theoretical basis for taking a practical training on the TEM. This course provides a comprehensive introduction to transmission electron microscopy (TEM) in the field of materials science. For an instrument operated by a single user, modern TEM provides an analytical platform with unsurpassed versatility, giving access to structural and chemical information from the micrometer to the sub-angstrom scale. In a thin, electron-transparent sample one can measure the crystallinity, grain structure, size, and defects, and the chemical composition. The crystal lattice can be imaged with atomic resolution, allowing observation of grain boundaries and interfaces. It is the only direct structural analysis method for studying nanoparticles. With this course you will gain a deep understanding of modern TEM and the connection between: - the optics and operation of the instrument; - the physics of electron-matter interactions; - insights into the materials properties of the sample. This gives the background to: - identify TEM techniques suitable to solving specific scientific problems; - interpret TEM data presented in articles; appreciate the impact of technological advances that have, for instance, led to sub-angstrom resolution by aberration correction. It can also be the basis for subsequent practical training on this remarkable instrument, and a stepping stone towards learning very advanced techniques with magical names like “dark field holography” or “angular resolved electron energy-loss spectroscopy”. Recommended background: Basics of crystallography and diffraction, college optics (construction of ray diagrams) are absolutely mandatory prerequisites; Fourier optics, more advanced crystallography and solid state physics are of great advantage.

Навыки, которые вы освоите

Materials scienceSchematic DiagramselectromagneticsAnalytical TestingApplied MathematicsLaboratory EquipmentEngineering, Scientific, and Technical InstrumentsLaboratory ResearchScientific VisualizationPhysicsChemistry

Программа курса

8 модулей · 125 учебных материалов

01Introduction21 материалов

Welcome

WelcomeЧтениеWelcome from the teacherВидеоDiscussion forumsЧтениеGrading policy and certificateЧтение

Учитесь у экспертов

Cécile Hébert

Prof.

Duncan Alexander

Dr.

Transmission electron microscopy for materials science
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Обучение на Coursera

≈ 45.9 ч

8 модулей

Язык: Английский

Субтитры: Испанский, Русский, Французский

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External resourcesЧтение
Where to get helpЧтение

Lesson 1.1: History, constituents of TEM

Week 1 introductionЧтениеSection 1.1ЧтениеAwareness Quiz 1.1ЗаданиеIntroduction: the instrument - I. History and building blocksВидеоReminders! Ray Diagrams.ВидеоExercises for lesson 1.1ЧтениеControl Quiz 1.1ЗаданиеFurther resourcesЧтение

Lesson 1.2: Lens aberrations

Section 1.2ЧтениеAwareness QuizЗаданиеLens aberrationsВидеоExercises for lesson 1.2ЧтениеControl Quiz 1.2ЗаданиеAssignment Week 1Взаимная проверкаYour feedbackPLUGIN
02Introduction (II)15 материалов

Lesson 2.1: Block of lenses

Week 2 introductionЧтениеSection 2.1ЧтениеAwareness Quiz 2.1ЗаданиеThe instrument - II: description of the 3 main blocksВидеоQuiz-video: 3-lens condenser systemВидеоExercises for lesson 2.1ЧтениеControl Quiz 2.1Задание

Lesson 2.2: The TEM put together

Section 2.2ЧтениеAwareness Quiz 2.2ЗаданиеBragg's LawВидеоTEM in operationВидеоExercises for lesson 2.2ЧтениеControl Quiz 2.2ЗаданиеAssignment Week 2Взаимная проверка
03Diffraction basics (I): Ewald sphere / Reciprocal lattice19 материалов

Lesson 3.1: 2-beam electron diffraction

Week 3 introductionЧтениеSection 3.1ЧтениеAwareness Quiz 3.1Задание3.1: 2-beam electron diffractionВидеоNote on Miller indices (h k l)ЧтениеExercises for Lesson 3.1ЧтениеControl Quiz 3.1Задание

Lesson 3.2: Reciprocal lattice

Section 3.2ЧтениеAwareness Quiz 3.2ЗаданиеReciprocal latticeВидеоExercises for Lesson 3.2ЧтениеControl Quiz 3.2Задание

Lesson 3.3: the Ewald sphere

Section 3.3ЧтениеAwareness Quiz 3.3ЗаданиеEwald sphere constructionВидеоExercises for Lesson 3.3ЧтениеControl Quiz 3.3ЗаданиеAssignment Week 3Взаимная проверкаYour feedback
04Diffraction basics (II): Multi-beam / Kinematical scattering18 материалов

Lesson 4.1: Multiple beam diffraction

Week 4 introductionЧтениеSection 4.1ЧтениеAwareness Quiz 4.1ЗаданиеMultiple beam scatteringВидеоExercises for Lesson 4.1ЧтениеControl quiz 4.1Задание

Lesson 4.2: Shape effects in reciprocal lattice

Section 4.2ЧтениеAwareness Quiz 4.2ЗаданиеShape effects on reciprocal latticeВидеоExercises for Lesson 4.2ЧтениеControl Quiz 4.2Задание

Lesson 4.3: Deviation from Bragg scattering

Section 4.3ЧтениеDeviation from Bragg scatteringВидеоReferencesЧтениеExercises for lesson 4.3ЧтениеControl Quiz 4.3ЗаданиеAssignment Week 4Взаимная проверкаYour feedback
05Diffraction and imaging: Dynamical effects (I)12 материалов

Dynamical scattering

Week 5 introductionЧтениеSection 5.1ЧтениеDynamical scatteringВидеоAddendum: Notations for dynamical scatteringВидеоExercises for Lesson 5.1ЧтениеControl Quiz 5.1Задание

Thickness fringes

Section 5.2ЧтениеThickness fringesВидеоExercises for Lesson 5.2ЧтениеControl Quiz 5.2ЗаданиеAssignment Week 5Взаимная проверкаYour feedbackPLUGIN
06Diffraction and imaging: Dynamical effects (II)11 материалов

Bend contours

Week 6 introductionЧтениеSection 6.1ЧтениеBend contoursВидеоExercises for Lesson 6.1ЧтениеControl Quiz 6.1Задание

Double diffraction

Section 6.2ЧтениеDouble diffractionВидеоExercises for Lesson 6.2ЧтениеControl Quiz 6.2ЗаданиеAssignment Week 6Взаимная проверкаYour feedbackPLUGIN
07Phase contrast (I)14 материалов

Contrast transfer function

Week 7 introductionЧтениеSection 7.1ЧтениеAwareness quiz.ЗаданиеMatch fourier transform to functionPLUGINIntroductionВидеоContrast Transfer FunctionВидеоExercises for week 7.1ЧтениеControl Quiz 7.1Задание

Weak phase object approximation

section 7.2ЧтениеWeak phase object approximationВидеоExercises for week 7.2ЧтениеControl Quiz 7.2ЗаданиеAssignment Week 7Взаимная проверкаYour feedbackPLUGIN
08Phase contrast (II)15 материалов

Phase contrast transfer function

Week 8 introductionЧтениеSection 8.1ЧтениеAwareness QuizЗаданиеInstallation of JEMS student editionЧтениеPhase Contrast Transfer FunctionВидеоPython notebook for the PCTFЛабораторнаяExercises for week 8ЧтениеControl Quiz 8.1Задание

HRTEM

Section 8.2ЧтениеHRTEMВидеоExercisesЧтениеControl Quiz 8.2ЗаданиеAssignment Week 8Взаимная проверкаConclusionВидеоYour feedbackPLUGIN
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